中药巴戟天中水溶性多糖的分离及结构鉴定

天然产物研究与开发 ›› 2011, Vol. 23 ›› Issue (1): 1-5.

• 研究论文 • 下一篇

中药巴戟天中水溶性多糖的分离及结构鉴定

杨振民^1,2，伊勇涛²，高川川²，范坚强³，胡军²，赵明月^2*

¹中国科学院大连化学物理研究所国家色谱中心，大连 116023；²中国烟草总公司郑州烟草烟草院香精香料研究室，郑州450001；³ 龙岩烟草工业有限责任有限公司，龙岩364021

收稿日期:2010-03-22 发布日期:2011-07-20
通讯作者: mingyuezhao58@126.com

Isolation and Identification of a Water-soluble Polysaccharide from Morinda officinalis

YANG Zhen-min^1,2, YI Yong-tao², GAO Chuan-chuan², FAN Jian-qiang³, HU Jun², ZHAO Ming-yue^2*

¹National Chromatographic R&A Center, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, China; ²Laboratory of Flavor & Fragrance, Zhengzhou Tobacco Research Institute of CNTC, Zhengzhou 450001, China; ³Longyan Tobacco Industrial Co., Ltd. Longyan 364021, China

Received:2010-03-22 Published:2011-07-20

摘要/Abstract

摘要：

中药巴戟天（Morinda officinalis）的根经过水提、醇沉、脱色和离子交换得到水溶性多糖（MOHP-1），经过FIIR、HPLC、NMR和GC-MS分析，最后确定MOHP-1是由果糖以(2→1)糖苷键连接的菊淀粉性多糖，其结构为α-Glcp-(1→2)-[β-Fruf-(2→1)-β-Frucf]_n。

关键词: 巴戟天, 多糖, 结构, FTIR, HPLC, NMR, GC-MS

Abstract:

A soluble polysaccharide (MOHP-1) was isolated from the roots of Morinda officinalis How via procedures including extraction, precipitation, deprotein, decolor and separation over anion-exchange. On the basis of FTIR, HPLC, NMR and GC-MS analysis after methylation, MOHP-1 was determined as α-Glcp-(1→2)-[β-Fruf-(2→1)-β-Frucf]_n, a polysaccharide with a linear chain of (2→1) linked β-fructofuranosyl residues specifying an inulin-type structure.

Key words: Morinda officinalis How, polysaccharide, structure, HPLC, NMR, GC-MS

中图分类号:

R284

杨振民，伊勇涛，高川川，范坚强，胡军，赵明月. 中药巴戟天中水溶性多糖的分离及结构鉴定[J]. 天然产物研究与开发, 2011, 23(1): 1-5.

YANG Zhen-Min, YI Yong-Tao, GAO Chuan-Chuan, FAN Jian-Qiang, HU Jun, ZHAO Ming-Yue. Isolation and Identification of a Water-soluble Polysaccharide from Morinda officinalis[J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2011, 23(1): 1-5.

参考文献

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中药巴戟天中水溶性多糖的分离及结构鉴定

Isolation and Identification of a Water-soluble Polysaccharide from Morinda officinalis

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