超声-微波协同皂化萃取茄尼醇条件的研究

天然产物研究与开发 ›› 2011, Vol. 23 ›› Issue (2): 291-294.

超声-微波协同皂化萃取茄尼醇条件的研究

鄢贵龙^*，刘爱云

淮阴师范学院江苏省环洪泽湖生态农业生物技术重点实验室，淮安 223300

收稿日期:2009-08-27 出版日期:2011-04-25 发布日期:2011-10-14
通讯作者: longygl@163.com
基金资助:
淮安市科技计划项目（SN0767）；淮阴师范学院青年优秀人才支持项目（06QNZC031）

Extraction of Solanesol by Ultrasonic-microwave Synergistic Saponification Method

YAN Gui-long^*, LUI Ai-yun

Jiangsu Key Laboratory of Eco-Agricultural Biotechnology around Hongze Lake, Huaiyin Normal University, Huaian 223300, China

Received:2009-08-27 Online:2011-04-25 Published:2011-10-14

摘要/Abstract

摘要：

实验研究了超声-微波协同皂化萃取茄尼醇的工艺条件，确定了其最适工艺参数为：在超声开的条件下，皂化时间60 min，微波功率40 W，氢氧化钠与烟叶浸膏的质量比为1:2，在此优化条件下茄尼醇皂化回收率为126.3%。与其它皂化法相比，超声-微波协同皂化萃取法具有节省时间、节约能量、茄尼醇回收率高等优点。

关键词: 茄尼醇, 超声-微波协同作用, 皂化

Abstract:

Ultrasonic-microwave synergistic saponification technique was applied to extract solanesol. The effects of main factors on saponification reaction were discussed and the optimum saponification conditions were as followed: the saponification time was 60 min，the microwave power was 40 W，the mass ratio of sodium hydroxide to tobacco extract was 1:2，and the ultrasonic was turned on. The results showed that under the optimized condition，the recovery rate of solanesol was 126.3%. Compared with other saponification methods，the ultrasonic-microwave synergistic saponification technique was a better method for solanesol extraction with less time and higher recovery rate of solanesol.

Key words: solanesol, ultrasonic-microwave synergistic saponification, saponification

鄢贵龙，刘爱云. 超声-微波协同皂化萃取茄尼醇条件的研究[J]. 天然产物研究与开发, 2011, 23(2): 291-294.

YAN Gui-Long, LIU Ai-Yun. Extraction of Solanesol by Ultrasonic-microwave Synergistic Saponification Method[J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2011, 23(2): 291-294.

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