响应面法优化树脂吸附红枣黄酮工艺研究

doi:A

天然产物研究与开发 ›› 2012, Vol. 23 ›› Issue (6): 808-.doi: A

响应面法优化树脂吸附红枣黄酮工艺研究

李治龙^1,2，刘新华²，刘文杰^*，冯婷¹

¹新疆塔里木大学生命科学学院；²塔里木盆地生物资源保护利用兵团重点实验室，阿拉尔 843300

收稿日期:2011-09-06 出版日期:2012-07-04 发布日期:2012-07-06

Optimization of Resins Adsorption Technology for Total Flavonoid from Jujube by Response Surface Methodology

LI Zhi-long^1,2, LIU Xin-hua², LIU Wen-jie^2*, FENG ting¹

¹College of Life Science, Tarim University, Alar 843300 Xinjiang; ²Key Laboratory of Biological Resource Protection and Utilization of Tarim Basin, Xinjiang Production & Construction Group, Alar 843300, China

Received:2011-09-06 Online:2012-07-04 Published:2012-07-06

摘要/Abstract

摘要： 以红枣为原料提取红枣黄酮，通过吸附树脂的筛选，探讨树脂吸附的溶液浓度、pH值、吸附时间、吸附液体积对树脂吸附条件的影响。利用Box-Behnken中心组合设计原理，应用响应曲面分析方法，确定了大孔吸附树脂对红枣黄酮最佳吸附条件为：最佳吸附树脂为XDA-8，吸附时间62 min，吸附液浓度为4.3 mg/L，pH值为7.32，吸附液体积为10 mL，最大吸附效率达到85.64%，优化后得实际吸附率为85.51%。

关键词: 树脂, 红枣, 响应面

Abstract: Adsorption and desorption characteristic of different resins for total flavonoid from Jujube was investigated. The experiment was conducted to study the effects of resin adsorption conditions on adsorption rate of flavonoid, and the adsorption time, pH, volume and concentration were developed. By the Box-Behnken centre united experiment design and response surface methodology, the optimum adsorption conditions were developed using resin XDA-8. The adsorption time was 62 min, volume value 10 mL, pH value 7.32 and the concentration was 4 mg/L. Under the optimum condition, the sample adsorption rate was 85.64%, and the actual rate of adsorption was 85.51%.

Key words: resin, Jujube, response surface methodology

中图分类号:

TS201.2

李治龙，刘新华，刘文杰，冯婷. 响应面法优化树脂吸附红枣黄酮工艺研究[J]. 天然产物研究与开发, 2012, 23(6): 808-.

LI Zhi-long, LIU Xin-hua, LIU Wen-jie, FENG ting. Optimization of Resins Adsorption Technology for Total Flavonoid from Jujube by Response Surface Methodology[J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2012, 23(6): 808-.

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响应面法优化树脂吸附红枣黄酮工艺研究

Optimization of Resins Adsorption Technology for Total Flavonoid from Jujube by Response Surface Methodology

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