河南和山西连翘叶中总木脂素、连翘酯苷A、连翘酯苷B和连翘苷的含量比较

doi:10.16333/j.1001-6880.2015.05.018

天然产物研究与开发 ›› 2015, Vol. 27 ›› Issue (5): 845-848.doi: 10.16333/j.1001-6880.2015.05.018

所属专题： No.7

河南和山西连翘叶中总木脂素、连翘酯苷A、连翘酯苷B和连翘苷的含量比较

原江锋1*，邱智军1，刘建利2，张志琪3

1 河南科技大学食品与生物工程学院，洛阳 471003；2 陕西省环境监测中心站，西安 710054；3 陕西师范大学化学化工学院，西安 710062

出版日期:2015-05-30 发布日期:2015-06-05

Determination of Total Lignans,Forsythiaside A,Forsythiaside B and Phillyrin in Forsythia suspensa Leaves from Henan and Shanxi

YUAN Jiang-feng1*, QIU Zhi-jun1, LIU Jian-li2, ZHANG Zhi-qi3

1 College of Food & Bioengingeering,Henan University of Science and Technology,Luoyang 471003,China; 2 Shannxi Environmental Center Monitoring Station,Xi’an 710054,China; 3 School of Chemistry & Chemical Engineering,Shaanxi Normal University,Xi’an 710062,China

Online:2015-05-30 Published:2015-06-05

摘要/Abstract

摘要： 测定河南和山西连翘叶中总木脂素、连翘酯苷A、连翘酯苷B和连翘苷含量。采用分光光度法测定连翘叶中总木脂素含量，结果显示山西连翘叶高于河南连翘叶总木脂素含量。采用高效液相色谱法（HPLC）测定连翘叶中连翘酯苷A、连翘酯苷B和连翘苷的含量。连翘酯苷A平均回收率为99.6%，RSD为1.23%；连翘酯苷B平均回收率为101.3%，RSD为1.74%；连翘苷平均回收率为102.3%，RSD为2.58%；连翘叶中连翘酯苷A和连翘苷的含量较高，并且不同产地连翘叶中连翘苷含量差异较大；另外对于富含连翘酯苷和连翘苷的连翘叶能否代替果实或者与果实合并用药有待于进一步研究。

关键词: 连翘叶, 总木脂素, 连翘酯苷A, 连翘酯苷B, 连翘苷

Abstract: The objective of this study was to determine the content of total lignans,forsythiaside A,forsythiaside B and phillyrin in Forsythia suspensa leaves from Henan province and Shanxi province.The total lignans of F.suspensa leaves from Shanxi province were higher than Henan province by spectrophotometry method.The contents of forsythiaside A,forsythiaside B and phillyrin were determined by HPLC.The average recoveries of forsythiaside A,forsythiaside B and phillyrin were 99.6% (RSD=1.23%),101.3% (RSD=1.74%) and 102.3% (RSD=2.58%),respectively.The experimental results showed that the content of forsythiaside A and phillyrin in F.suspensa leaves from Shanxi and Henan was relatively high.In addition,the content of phillyrin in F.suspense leaves from different habitats were of large difference. F.suspensa leaves are rich in forsythiaside and lignans,more researches on F.suspensa leaves are still needed to confirm whether it can be used as substitute or cooperate with F.suspensa fruit for medicinal application.

Key words: Forsythia suspensa leaves, total lignans, forsythiaside A, forsythiaside B, phillyrin

中图分类号:

Q946.91

原江锋1*，邱智军1，刘建利2，张志琪3. 河南和山西连翘叶中总木脂素、连翘酯苷A、连翘酯苷B和连翘苷的含量比较[J]. 天然产物研究与开发, 2015, 27(5): 845-848.

YUAN Jiang-feng1*, QIU Zhi-jun1, LIU Jian-li2, ZHANG Zhi-qi3. Determination of Total Lignans,Forsythiaside A,Forsythiaside B and Phillyrin in Forsythia suspensa Leaves from Henan and Shanxi[J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2015, 27(5): 845-848.

[1]	吕允珂, 郑萱, 张菊, 崔施展, 王明雪, 周春伶, 贾东升. 连翘叶总黄酮对斑马鱼溃疡性结肠炎的作用研究[J]. 天然产物研究与开发, 2024, 36(8): 1279-1287.
[2]	郭雪健, 李彬春, 赵邑, 尉敬涛, 张立伟. 人源肠道菌中转化连翘苷制备连翘脂素的菌株筛选及固定化[J]. 天然产物研究与开发, 2021, 33(12): 2090-2098.
[3]	原江锋1,2*，胡金婉1，王大红1,2，龚明贵1，李佩艳1. 不同产地连翘叶花中主要活性成分的含量分析[J]. 天然产物研究与开发, 2020, 32(3): 389-397.
[4]	李刚1, 魏庆红1, 段伟伟1. 一种新的连翘中连翘苷的HPLC含量测定方法[J]. 天然产物研究与开发, 2018, 30(增刊1): 137-140.
[5]	张元波1,2，张敏3，程启斌1，马丽莎1，张立伟1*. 连翘叶抗氧化谱效相关质量评价研究[J]. 天然产物研究与开发, 2017, 29(4): 629-634.
[6]	全云云，袁岸，龚小红，彭成，李芸霞. 连翘抗炎药效物质基础筛选研究[J]. 天然产物研究与开发, 2017, 29(3): 435-438.
[7]	刘建洲，张立伟*. 基于人呼吸道上皮细胞炎症模型的连翘提取物抗炎活性实验研究[J]. 天然产物研究与开发, 2015, 27(7): 1248-1253.
[8]	栗亚云，陈廷贵*，张立伟. 浊点萃取法结合超声波提取连翘叶中叶绿素[J]. 天然产物研究与开发, 2015, 27(2): 221-225.
[9]	刘伟霞，杨建雄. 基于响应面法从连翘叶中提取连翘酯苷A和连翘苷的工艺优化[J]. 天然产物研究与开发, 2012, 23(8): 1098-.

河南和山西连翘叶中总木脂素、连翘酯苷A、连翘酯苷B和连翘苷的含量比较

Determination of Total Lignans,Forsythiaside A,Forsythiaside B and Phillyrin in Forsythia suspensa Leaves from Henan and Shanxi

PDF (PC)

可视化

摘要/Abstract

引用本文

使用本文

参考文献

相关文章 9

编辑推荐

Metrics

本文评价