天然产物研究与开发 ›› 2017, Vol. 29 ›› Issue (增刊1): 106-112.doi: 10.16333/j.1001-6880.2017.S.023

• 开发研究 • 上一篇    下一篇

丹参热风干燥特性及动力学模型研究

杜利平1,2,刘伟1,王晓1,耿岩玲1,崔莉1*   

  1. 1 山东省中药质量控制技术重点实验室山东省分析测试中心,济南 250014;2山东农业大学 食品科学与工程学院,泰安 271018
  • 出版日期:2017-08-02 发布日期:2017-08-02

Hot-air drying characteristics and drying kinetics of Salvia miltiorrhiza Bunge

DU Li-ping1,2,LIU Wei1,WANG Xiao1,GENG Yan-ling1,CUI Li1*   

  1. 1 Key Laboratory of TCM Quality Control Technology,Shandong Analysis and Test Center Jinan 250014,China; 2College of Food Science and Engineering,Shandong Agricultural University,Taian 271018,China
  • Online:2017-08-02 Published:2017-08-02

摘要: 研究丹参的热风干燥特性、动力学模型及不同干燥条件下丹参中主要功效成分丹酚酸B和丹参酮ⅡA的含量变化。方法:在不同温度(50、60、70和80 ℃)下对不同直径(1.12、0.84和0.46 cm)的丹参进行热风干燥,得出相应的干燥曲线、干燥速率曲线,建立丹参不同干燥条件下的动力学模型,采用高效液相色谱法测定分析不同温度对干燥成品中丹酚酸B和丹参酮ⅡA含量的影响。结果:降速阶段为丹参热风干燥的主要阶段; Page 模型对丹参干燥过程的拟合性较好,模型的预测值与实验值吻合性好,可以用来描述和预测丹参的热风干燥失水过程;通过费克第二定律求出干燥过程中的水分有效扩散系数(Deff)在5.08389×1010~2.54195×109 m2/s范围内,且随着温度的升高而增大;通过阿伦尼乌斯方程计算出平均活化能为49.0967 KJ/mol;热风干燥温度宜选择50~70 ℃,此时干燥成品的丹酚酸B和丹参酮ⅡA含量较高。结论:丹参热风干燥的主要阶段为降速阶段,Page 模型适于预测和描述其失水过程,该研究结果对丹参实际生产具有一定的指导意义。

关键词: 丹参, 热风干燥, 动力学模型

Abstract: To study the hotair drying characteristics,drying kinetics mathematical models and the effect of different drying condition on the effective constituent,which included salvianolic acid B and tanshinoneⅡA of Salvia miltiorrhiza Bunge.Methods:The experiment was carried out at different hotair drying temperatures (50,60,70 and 80 ℃) and at different diameters (1.12,0.84 and 0.46 cm).The drying characteristics were detected and the drying kinetics mathematical model was established.Meanwhile,salvianolic acid B and tanshinoneⅡA were detected by highperformance liquid chromatography (HPLC).Results:The drying process occurred in falling rate periods;According to statistical parameters,the Page model predicts and describes the drying process more accurately than others.There was a good agreement between the experimental and predicted values of Salvia miltiorrhiza Bunge;The Fick’s second law of diffusion was employed to calculate the value of moisture effective diffusivity (Deff),which ranged from 5.08389 × 1010 ~2.54195 × 109m2/s,and increased with the increasing of drying temperature;The activation energy determined from Arrhenius equation was 49.0967 kJ/mol;The content of salvianolic acid B and tanshinoneⅡA is higher when the temperature rang 50 to70 ℃.Conclusion:The drying process of Salvia miltiorrhiza Bunge only contained deceleration stage.The Page model was the best suitable for predicting moisture ratio.The research results of Salvia miltiorrhiza Bunge has a certain guiding significance to practical production.

Key words: Salvia miltiorrhiza Bunge, hotair drying , kinetic modeling