天然产物研究与开发 ›› 2019, Vol. 31 ›› Issue (增刊2): 58-63.doi: 10.16333/j.1001-6880.2019.S.008

• 研究简报 • 上一篇    下一篇

苦水玫瑰花露中挥发性香气成分分析

雷春妮,王波,解迎双,周小平* ,孙苗苗,王亚琴   

  1. 兰州海关技术中心1,兰州 730010
  • 出版日期:2019-12-28 发布日期:2019-12-30
  • 基金资助:

    兰州海关科技计划(2017GK003);甘肃省科技支撑计划(1604NKCA079)

Analysis of volatile aroma components in Kushui rose water

LEI Chun-ni,WANG Bo,XIE Ying-shuang,ZHOU Xiao-ping*,SUN Miao-miao,WANG Ya-qin   

  1.  Lanzhou Customs Technology Center,Lanzhou 730010,China
  • Online:2019-12-28 Published:2019-12-30

摘要: 以苦水玫瑰花水为原料,分别采用液液萃取法、顶空法、固相微萃取法和吹扫捕集法提取玫瑰花水香气成分,使用气相色谱-质谱法(GC-MS)结合MassworksTM质谱解析软件鉴定分析,结果表明,吹扫捕集法因提取效果好、操作简单、重复性好、绿色环保、自动化程度高等优点,更适用于玫瑰花露香气成分的批量快速分析。玫瑰花水和细胞液共鉴定出香气成分74种,其中玫瑰花水70种,细胞液67种;玫瑰花水和细胞液共有成分62种,相对含量之和分别为81.17%、90.75%;玫瑰花水特有成分7种,相对含量之和为5.90%,细胞液特有成分4种,相对含量之和为1.45%。玫瑰花水和细胞液香气成分存在差异。

关键词: 玫瑰花水, 细胞液, 香气, 吹扫捕集-气相色谱/质谱联用技术

Abstract: The Kushui rose water was used as the raw material to extract the aroma components of rose water by liquid-liquid extraction,headspace method,solid phase microextraction and purging and trapping,respectively.Gas chromatography-mass spectrometry (GC-MS) was combined with MassworksTM.The identification analysis of mass spectrometry software shows that the purging and trapping method is more suitable for batch rapid analysis of rose aroma components because of its good extraction effect,simple operation,good repeatability,green environmental protection and high degree of automation.A total of 74 kinds of aroma components were identified in rose water and cell fluid,including 70 kinds of rose water and 67 kinds of cell fluid.There are 62 kinds of ingredients in rose water and cell fluid,and the relative content is 81.17% and 90.75% respectively.There are 7 unique components of rose water,the sum of relative contents is 5.90%,the unique components of cell fluid are 4,and the sum of relative contents is 1.45%.There was a difference between rose water and cell liquid aroma components.

Key words: rose water, cell fluid, aroma, purging and trapping-gas chromatography/mass spectrometry

中图分类号: 

S573.7 O657.7