天然产物研究与开发 ›› 2018, Vol. 30 ›› Issue (增刊2): 57-63.

• 研究论文 • 上一篇    下一篇

ICP-OES法测定水母雪兔子不同部位21种元素含量

栾真杰1,2,李佩佩1,2 ,陈保政1,2,周玉碧1,万丽娜1,2,卢学峰1,孙菁1*   

  1. 1青海省青藏高原特色生物资源研究重点实验室 中国科学院西北高原生物研究所,西宁 810008;2中国科学院大学,北京 100049
  • 出版日期:2019-01-18 发布日期:2019-01-18
  • 基金资助:

    国家自然科学基金青年基金(81403051);青海省重点实验室发展建设专项(2017-ZJ-Y10);青海省自然科学基金面上项目(2016-ZJ-955);青海省创新平台建设专项项目(2017-GX-G03);西宁市重点研发与转化计划(2018-Y-59)

Determination of 21 Mineral Elements in Different Parts of Saussurea medusa Maxim.by ICP-OES

LUAN Zhen-jie1,2,Li Pei-pei1,2,CHEN Bao-zheng1,2,ZHOU Yu-bi1,WAN Li-na1,2,LU Xue-feng1,SUN Jing1*   

  1. 1Qinghai Key Laboratory of Qinghai-Tibet Plateau Biological Resources,Northwest Institute of Plateau Biology,Chinese Academy of Sciences,Xining 810008,China; 2Graduate University of Chinese Academy of Sciences,Beijing 100049,China
  • Online:2019-01-18 Published:2019-01-18

摘要: 本文采用电感耦合等离子体原子发射光谱法(ICP-OES)对水母雪兔子不同部位中的21种矿质元素的含量进行了测定,利用微波消解法处理目标植物。结果显示,所有部位均未检出Mo,花中未检出Co和Cd。从植株整体上来看,水母雪兔子以Cr、Mn、Pb、Se、Sr、Cu、Ni、Zn这8种元素最具有代表性,为其特征元素。水母雪兔子中含有丰富的钙和镁,8种人体必需微量元素中水母雪兔子含有最多的是铁元素,其中又以叶中含量居多,其余所测人体必需微量元素含量中,根据变异系数,四个部位中含量差异最小的是Se元素(CV=1.13),含量差异最大的是Cr元素(CV=118.52),几乎不含有Co元素。该植物四个部位之间元素含量存在一定差异。通过探讨该雪莲植物中元素分布特征及差异,旨在为该植物资源药效物质基础深入研究和后续资源的深度开发利用提供一定的科学依据。

关键词: 水母雪兔子, ICP-OES法, 元素含量, 因子分析

Abstract: Saussurea medusa Maxim. is a rare Chinese medicine,this study is to determine the content and distribution of elements in Saussurea medusa Maxim. to provide a basis for its utilization.The plants were digested by nitric acid microwave.The 21 elements in different parts of the plants was determined by inductively coupled plasma optical emission spectrometry (ICP-OES).The data were analyzed by Solutions Statistical Package for the Social Sciences 22.0 (SPSS 22.0).The method for the determination of 21 elements in four different parts of the plant was established.No Mo was detected in all four parts,Co and Cd were not detected in the flowers.For the whole plant,the eight elements of Cr,Mn,Pb,Se,Sr,Cu,Ni,and Zn are the most representative.Among the 11 essential elements required by the human body,the Saussurea medusa Maxim. is rich in Ca and Mg.Among the eight essential trace elements,Saussurea medusa Maxim. contains the most Fe,which is the most abundant in the leaves.Among the other trace elements which are necessary for human,Se is of the smallest difference among the four parts,the largest one is the Cr,and almost no Co.The established detection method is accurate,reliable and high precision.It’s suitable for analyzing the elemental content of plants.There are some differences in the content of elements between the four parts of the plant,which can provide a scientific basis for further study.

Key words: Saussurea medusa Maxim., ICP-OES, mineral elements, factor analysis

中图分类号:  O657.3