天然产物研究与开发 ›› 2011, Vol. 23 ›› Issue (1): 82-84.

• 研究简报 • 上一篇    下一篇

新疆洋海古代大麻叶的大麻酚分析

马青云1,2,蒋洪恩3,赵友兴1*   

  1. 1中国科学院昆明植物研究所植物化学与西部植物资源国家重点实验室,昆明 650204;2云南科技信息职业学院,昆明 650224;3中国科学院植物研究所,北京 100093

  • 收稿日期:2009-05-15 发布日期:2011-07-20
  • 通讯作者: yxzhao@mail.kib.ac.cn

Analysis of Cannabinoids from Leaves of Ancient Cannabis sativa Found in Yanghai Xinjiang, China

MA Qing-yun1,2, JIANG Hong-en3, ZHAO You-xing1*   

  1. 1State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute of Botany, Chinese Academy of Sciences, Kunming 650204, China; 2Yunnan Institute of Technology & Information, Kunming 650224, China; 3Institute of Botany, Chinese Academy of Sciences, Beijing 100093, China

  • Received:2009-05-15 Published:2011-07-20
  • Supported by:

    This work was supported by the National Natural Science Foundation of China (40403014).

摘要:

为了检测新疆吐鲁番地区洋海古墓中2500年前大麻叶中两个大麻酚:四氢大麻酚(THC)与大麻二酚(CBD),采用高压液相分析技术(HPLC)测定26.716 g大麻叶中THC与CBD的含量分别为0.2928 mg与0.2830 mg,占叶重量的(0.110%)%与(0.106%)%。THC与CBD标准品从现代大麻叶中分离得到,通过波谱分析鉴定。

关键词: 大麻, 大麻酚, 分析

Abstract:

To detect two cannabinoids, delta-9-tetrahydro cannabinol (THC) and cannabidiol (CBD) from the leaves of 2500-year-preserved Cannabis sativa unearthed from Yanghai Tombs, Turpan District in Xinjiang, China, high performance liquid chromatogram (HPLC) analysis showed that the amounts of THC and CBD determined from 26.716 g leaves of 2500-year-preserved C. sativa were 0.2928 mg and 0.2830 mg, which covered 0.110%% and 0.106%% of dried materials, respectively. The authentic samples of THC and CBD were isolated from extant leaves of C. sativa and were elucidated on the basis of spectroscopic analysis.

Key words: Cannabis sativa, cannabinoids, analysis