天然产物研究与开发 ›› 2010, Vol. 23 ›› Issue (6): 1040-1044.

• 研究简报 • 上一篇    下一篇

鞑靼滨藜挥发性化学成分分析

Janar  Jenis1,G. Sh Burasheva1,阿吉艾克拜尔•艾萨2*,巴 杭2,Zh. A Abilov1   

  1. 1哈萨克斯坦国立大学化学系,阿拉木图 050012;2中科院新疆理化技术研究所,乌鲁木齐 830011
  • 收稿日期:2008-12-30 出版日期:2011-01-10 发布日期:2011-10-19
  • 通讯作者: haji@ms.xjb.ac.cn
  • 基金资助:

    新疆植物资源化学重点实验室开放课题(2008-04)

Volatile Constituents from Atriplex tatarica

Janar  Jenis1,G. Sh Burasheva1,Haji Akber Aisa 2,BA Hang2,Zh. A Abilov1   

  1. 1Chemistry Department of al-Farabi Kazakh native University, Almaty 050012, China; 2Xinjiang Technical Institute of Physics and Chemistry, Urumchi 830011, China
  • Received:2008-12-30 Online:2011-01-10 Published:2011-10-19

摘要:

对鞑靼滨藜全草的挥发性化学成分进行分析。采用水蒸气蒸馏法及索氏提取法提取鞑靼滨藜全草中的挥发性化学成分,用GC-MS 联用技术分析其化学组成,计算其相对百分含量,并对两种提取方法进行比较研究。结果表明:水蒸气蒸馏法提取物的成分比索氏提取法较多。从水蒸气蒸馏法分离出的53个色谱峰中鉴定了51种成分,含量最高的是茴香脑(45.84%),其次为正二十七烷(9.28%),羟基吲哚(6.81%),α-羟基-2-甲基丙基苯乙酸酯(4.03%)。从索氏提取法分离出的26个色谱峰中鉴定了22种成分,含量最高的是正二十九烷(22.63%),其次为硬酯酸(16.69%),十六醛(6.89%),棕榈酸(5.43%)。

关键词: 鞑靼滨藜, 挥发性化学成分, 水蒸气蒸馏法, 索氏提取法

Abstract:

The volatile oils extracted from the whole plants of Atriplex tatarica by water steam distillation and Soxhlet extraction were analyzed by GC-MS. The relative content of each component was determined by area normalization. Fifty-three compounds were separated and fifty-one of them were identified from the oil of water steam distillation method, the major constituents are 1-methoxy-4-(1-propenyl)-benzene (45.84%), heptacosane (9.82%), 1H-indol-5-ol (6.81%), benzenacetic acid, ?α-hydroxy-, and 2-methylpropyl ester (4.03%). Twenty-six compounds were separated and twenty-two of them were identified from the oil of Soxhlet extraction method, the major constituents are nonacosane (22.63%), (z,z)-9,12-octadecanoic acid (16.69%), hexadecanal (6.89%), and n-hexadecanoic acid (5.43%).

Key words: Atriplex tatarica, volatile constituents, GC-MS