Abstract: Ten phenylpropanoid derivatives were isolated and purified from EtOAc fraction of 70% ethanol extract of Callicarpa macrophylla Vahl by silica gel,Sephadex LH-20 and ODS column chromatography.On the basis of their physico-chemical properties and spectroscopic data,these compounds were identified as balanophonin (1), (7R, 8S)-dehydroconiferyl alcohol-8,5′-dehydroconiferyl aldehyde-9-O-β-D-glucopyranoside (2), forsythoside B (3),alyssonoside (4),leucosceptoside B (5),acteoside (6),martinoside (7),isoacteoside (8),plantainoside C (9),isomartynoside (10).Compounds 3-10 were isolated from this plant for the first time.

Key words: Verbenaceae, Callicarpa macrophylla Vahl, phenylpropanoid derivatives, chemical constituents