Volatiles in Buds and Flowers of Forsythia suspense

Abstract

Abstract:

The volatile constituents from the buds and flowers of Forsythia suspense were analyzed by head-space solid phase microextraction,coupled with GC-MS. Eighty-three compounds were identified from the buds and flowers of F. suspense, and 40 compounds were mutual. Hydrocarbons (41.04%) were the main constituents in the buds and alcohols, aldehydes and ketones (26.46%) were dominant in the flowers. Esters decreased from 8.11% in buds to 2.12% in flowers, and acids increased from 3.56% in buds to 5.18% in flowers. It indicated that esters were hydrolyzed into acids with blooming.

Key words: solid-phase microextraction, Forsythia suspense, volatile constituents

CLC Number:

WANG Jin-mei, JI Zhi-qiang, KANG Wen-yi. Volatiles in Buds and Flowers of Forsythia suspense[J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2011, 23(3): 458-463.

References 8

1	Wang JM(王金梅),Xu QT(许启泰),Kang WY(康文艺).Research progress on chemical components and the pharmacology of Forsythia suspense (Thunb.)Vahl.Natl Prod Res Dev(天然产物研究与开发),2007,19 :153-157.
2	Xu ZL(徐植灵),Pan JG (潘炯光),Ji L(吉力),et al.Studies on essential oils of Forsythia suspense.Natl Prod Res Dev(天然产物研究与开发),1994,6(1):14-17.
3	Kong J(孔杰),Yao J(姚健),Da WY(达文燕),et al.Studies on essential oils of Forsythia suspense.J Northwest Normal Univ Nat Sci (西北师范大学学报,自科版),2001,37 (4):77-81.
4	Hao XL (郝旭亮),刘霞 (Liu X),倪艳 (Ni Y),et al.GC-MS comparison of essential oil from Forsythia suspense extracted by two different methods.Chin Tradit Patent Med(中成药),2002,24:534-536.
5	Wu JF(武建芳),Lu X(路鑫),Tang WY(唐婉莹),et al.Comprehensive two-dimensional gas chromatography/ time-of-flight mass spectrometry for the analysis of Forsythia suspense volatile oil.J Chin Nat Med(中国天然药物),2003,1(3):150-154.
6	He XX(何新新),Wang YP(王伊鹏),Wu Z(吴忠),et al.Analysis of essential oils of Forsythia suspense from different area.J Chin Med Mat(中药材),2000,23:397-398.
7	Lv JS (吕金顺),Liu XY (刘晓英).Study on chemical constituents of essential oil of flowers of Forsythia suspense (Thunb.) Vahl.J Chin Spe Lab(光谱实验室),2004,21:815-817.
8	Wang JM(王金梅),Xu QT(许启泰),Kang WY(康文艺).The volatile oil from different parts of Lonicera japonica Thunb.Fine Chem(精细化工),2008,25:1075-1078.

[1]	FENG Yan-zhi, YANG Chao-wei, WANG Bao-ping, QIAO Jie, ZHOU Hai-jiang, ZHAO Yang. Determination of volatile components in the flowers of different Paulownia species based on HS-SPME and GC-MS [J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2023, 35(7): 1163-1171.
[2]	ZHANG Xin-yi, JIANG Han-mei, CHENG Li, LIU Yi. HS-SPME-GC-MS analysis of the changes in volatile components before and after the compatibility of Radix Bupleurum and Radix Paeoniae Alba [J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2023, 35(11): 1907-1914.
[3]	YI Zi-rong, ZHANG Rui-ying, WANG Jia-ling, LI Ke-ai, ZHANG Yu-xiang, CHEN Miao-feng, ZHENG Ya-jie, TANG Qi. Determination of volatile components in different parts of Atractylodes macrocephala Koidz. by HS-SPME-GC-MS [J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2022, 34(10): 1690-1698.
[4]	LUO Lin, YUAN An, DANG Jue, ZHAO Meng-jie, LI Yun-xia. Antipyretic and Anti-inflammatory Effects of Forsythia suspense* Volatile Oil in Different Rats Models [J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2018, 30(2): 207-211.
[5]	TIAN Ding, SHI Meng-qi, WANG Yun. Volatile Oil from Forsythia suspense: Chemical Constituents and Pharmacological Effects [J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2018, 30(10): 1834-1842.
[6]	WANG Ya-ru,LI Ya-meng,YANG Na,ZHOU Bai-song,LI Ping-ya,LIU Jin-ping. Nalysis of Volatile Components in Sonchusarvensis* L.by HS-SPME/GC-MS [J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2017, 29(增刊2): 241-245.
[7]	WU Chao-ran1, FANG Xian-ying1, XIAO Wei2. Review on Non-volatile Components and Pharmacological Activity of Osmanthus fragrans [J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2017, 29(8): 1439-1448.
[8]	ZHANG Yuan-bo1,2,ZHANG Min3, CHENG Qi-bin1,MA Li-sha1,ZHANG Li-wei1*. Relationship Between HPLC Fingerprint Chromatogram and Antioxidant Activity of Forsythia suspense Leaves [J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2017, 29(4): 629-634.
[9]	. Study on Agarwood ‘Qinan’ in Yuenan by GCMS [J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2016, 28(Suppl1): 35-38.
[10]	YU Xiao1, PAN Wei-song1, TIAN Hao1,2, WANG Jian-wen1. Effect of Salt Stress on Growth of Artemisia annua* L. and Its Volatile Metabolites [J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2015, 27(9): 1539-1543.
[11]	ZHANG Wei1, ZHU Xiao-di2, ZHANG Juan-juan1, ZHANG Yong1, YIN Zhen-hua1. Contrastive Analysis of Volatile Components in Leaves and Flowers of Psophocarpus tetragonolobus* (Linn.) DC. [J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2015, 27(10): 1732-1736.
[12]	XUE Peng, ZHANG Dong, YANG Li-xin, CAO Ying-xi, YANG Lan. Study on the Volatile Constituents of Hedyotis corymbosa* (L.)Lam.by SPME-GC/MS [J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2014, 26(Suppl1): 34-37.
[13]	LIU Wei-xia, YANG jian-xiong. Optimization of Extraction Technology of Forsythiaside and Phillyrin in Forsythia suspense Leaves Based on Response Surface Methodology [J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2012, 23(8): 1098-.
[14]	TIAN Pu-yu, LI Chang-qin, WANG Jin-mei, KANG Wen-yi. Volatiles in Clerodendron trichotomum Thunb.by Head-Space Solid Micro-Extraction Coupled with GC-MS [J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2011, 23(6): 1077-1079.
[15]	GAO Guang-chun,ZHENG Xu-song,XU Hong-xing,LU Zhong-xian. Analysis of Volatile Compounds from Melinis minutiflora by HS-SPME-GC-MS [J]. NATURAL PRODUCT RESEARCH AND DEVELOPMENT, 2011, 23(6): 1073-1076.