NATURAL PRODUCT RESEARCH AND DEVELOPMENT ›› 2014, Vol. 26 ›› Issue (3): 374-379.

• Article • Previous Articles     Next Articles

Analysis of Volatile Components from Pterocarpus indicus Leaves with Different Extraction Methods by Gas Chromatography-Mass Spectrometry

ZHENG Li-xia1, GAO Ze-zheng2, WU Wei-jian1*, LIANG Guang-wen1, FU Yue-guan3   

  1. 1 Laboratory of Insect Ecology,South China Agricultural University,Guangzhou 510642,China; 2 South China Botanical Garden,Chinese Academy of Sciences, Guangzhou 510520,China; 3 Environment and Plant Protection Institute, Chinese Academy of Tropical Agricultural Sciences,Danzhou,Hainan 571737,China
  • Online:2014-03-29 Published:2014-12-08

Abstract: The volatile components from Pterocarpus indicus leaves were extracted by simultaneous distillation extraction (SDE),solid phase micro-extraction (SPME) and dynamic headspace adsorption (DHA) and analyzed using gas chromatography-mass spectrometry (GC-MS).The results indicated that the volatile oil compounds extracted out using the three methods were different.Twenty-five chemical components were identified from the SDE extract,the main component was 2-nitroethanol, accounting for 35.29% of the total identified components;Twenty-seven chemical components were identified from the SPME extract,the main component was cis-3-hexenyl-1-acetate,accounting for 33.62% of the total identified components;Twenty-seven chemical components were identified from the DHA extract,the main component was 2-nitroethanol,accounting for 30.42% of the total identified components.Two compounds were detected in all the three extracts.In addition, alcohols,esters and acetals were the major components detected in all the three extracts.

Key words: Pterocarpus Indicus, simultaneous distillation extraction, solid phase micro-extraction, dynamic headspace adsorption, gas chromatography-mass spectrometry

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